Canada Carbon announces positive results from graphite half-cell battery testing with Polaris Battery Labs, LLC.
February 22 2024 - 6:00PM
Canada Carbon Inc. (the "Company" or "Canada
Carbon" or "CCB") (TSX-V:CCB),(FF:U7N1) is pleased to announce it
has successfully completed half-cell battery testing of its
graphite material with Polaris Battery Labs, LLC (“Polaris”). Flake
graphite provided for this testing was provided from Canada Carbons
Miller Graphite Mine project (Miller) located in
Grenville-sur-la-Rouge, Quebec.
Coin cells for Canada Carbon were assembled and
tested by Polaris Battery Labs against a commercially available
graphite baseline material for comparison. Both sets of cells were
assembled using a lithium metal counter electrode, Wattman glass
fiber separator and 1M LiPF6 in 3:7 EC:EMC electrolyte. The coin
cells were tested according to Polaris' Batch Qualification regime
to determine the first cycle loss, reversible capacity, and other
key electrochemical parameters.
Canada Carbons flake graphite material showed
promising results in terms of capacity and first cycle loss in
comparison to commercial baseline materials with ~6.5% first cycle
loss and 353mAh/g reversible capacity which is above the commercial
reference graphite material testing at an average 345mAh/g. Data
indicates that improvements in rate performance are still needed to
achieve commercial performance, however this can be attributed to
flake graphite being used in comparison to commercially used CSPG
(coated, spheroidized, purified graphite) which allows lithiation
only on the edge plane leading to typically slower lithiation and
delithiation rate capabilities. However, improvements in
performance would likely be seen with additional post processing
such as spheroidization and pitch coating which are used in
commercial materials today.
Doug Morris, CEO and Director of Polaris Labs,
stated: “These initial results from half-cell (coin cell) testing
confirm excellent graphite properties. Given these positive
results, we will now progress into testing of full pouch cells.
These tests confirm that the Canada Carbon graphite material is
suitable for anode material and electrode/battery markets. Canada
Carbon and Polaris will continue the test program through out
2024.”
Highlights of this Study
Cell Materials and Testing:
- 8.89 mg/cm² mass loading calendared
to 1.56 g/cm³
- 304SS CR2032 coin cell cans
- Whatman GF/F separator
- 200 µm (fully compressed) glass
fiber material used to separate the graphite anode from the lithium
reference/counter electrode.
- 1.0 M LiPF6 in 3:7 EC:EMC
electrolyte (Polaris Standard)
- Testing:
- Estimated Cell Capacity: 5.82
mAhr
- Formation: CC Dchg/Chg @ C/20
- Cycle: CCCV Dchg/CC Chg w/ C/20 CV
@ C/10, C/5, C/2, and C/10 (3x each rate)
- Formulation
- Graphite – 94.5%
- Imerys C65 – 1.5%
- Wealthy Chem BH-1000 CMC –
1.5%
- MTI SBR (dry basis) – 2.5%
- Mix Solids – 41.88%
- Mix Viscosity – 2,930 mPa*s
- FoG (Hegman) –
no legible reading obtained.
Electrochemical Results:
- Irreversible capacity (first cycle
loss) – 6.53% average
- Reversible delithiation capacity @
C/10 – ~353 mAh/g
- Stabilized capacity at final C/10
cycles
- Theoretical graphite capacity – 372
mAh/g
- Capacity stable up to C/2
- Cycling
efficiency improvement
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“These results are quite promising and
demonstrate the capabilities of Canada Carbon’s graphite to meet
the needs of battery producers. We fully expect performance to
improve significantly as post processing activities
(spheroidization, pitch coating, etc) occur for this specific
material”, notes Shelly Whitlock, CEO for Iridian Labs.
Ellerton Castor, CEO of Canada Carbon shared ”We
are encouraged by the positive electrochemical testing results of
Miller flake graphite concentrate. This phase of testing with
Polaris confirms our hypothesis about Miller: that the high quality
and purity of the flake makes it well suited for applications
beyond the nuclear power vertical. The implications for commercial
scalability of the Miller deposit are far-reaching. With additional
upgrading, such as spheroidization, we are confident that these
improvements will give us the performance needed to have a deliver
a premium product to the battery market.“
About Canada
CarbonCanada Carbon, Inc. is a Canadian
mining company developing multiple natural graphite deposits geared
to the Green Economy. CBB holds a 100% interest in two past
producing graphite mines, the Miller and the Asbury mines, both
located in Quebec. The Miller hydrothermal lump-vein historical
graphite mine and surrounding property cover approximately 100
square kilometres (km)2 and is located 80 km west of Montreal
in the township of Grenville-sur-la-Rouge. The Asbury Graphite Mine
a past producing property made up of 25 active claims for a total
of 1,384.59 hectares or 13.8 km2. It is located
8.1km northeast of Notre-Dame-Du-Laus in the Laurentides Region of
southern Quebec.
About IridianIridian is a
graphite R&D company tailored to the needs of the battery
industry. Iridian provides batch qualification services including
lab scale post graphite mining processing (I.e. spheroidization,
graphitization and pitch coat), material characterization testing,
and electrochemical assessments. Iridian’s graphite and battery
expertise provides the key connection between the raw purified
mined graphite material and a product that is ready for global
battery markets.
About Polaris LabsPolaris will
help you to navigate to your destination to commercialize your new
materials and technologies. We’ll build and test your cells to see
how they perform. We’ll engineer processes for your next-generation
technologies and offbeat ideas. We’ll be your battery consultants.
Basically, we’re your experts for designing, building, and testing
the materials and cells that will one day make up the batteries
powering our world.
CANADA CARBON INC. “Ellerton
Castor”Chief Executive Officer and Director Contact Information
E-mail inquiries: info@canadacarbon.com P: (905)
407-1212
FORWARD LOOKING INFORMATION
This press release contains statements that constitute
“forward-looking information” (“forward-looking information”)
within the meaning of the applicable Canadian securities
legislation. All statements, other than statements of historical
fact, are forward-looking information and are based on
expectations, estimates and projections as at the date of this
press release. Any statement that discusses predictions,
expectations, beliefs, plans, projections, objectives, assumptions,
future events or performance (often but not always using phrases
such as “expects”, or “does not expect”, “is expected”,
“anticipates” or “does not anticipate”, “plans”, “budget”,
“scheduled”, “forecasts”, “estimates”, “believes” or “intends” or
variations of such words and phrases or stating that certain
actions, events or results “may” or “could”, “would”, “might” or
“will” be taken to occur or be achieved) are not statements of
historical fact and may be forward-looking information.
Forward-looking information in this press release includes
statements regarding the development of the Company’s Miller
deposit and financing thereof, the entering of the joint venture
with Irondequoit Offering, future production from the Company’s
Miller deposit, sales agreements and other matters related thereto.
In disclosing the forward-looking information contained in this
press release, the Company has made certain assumptions. Although
the Company believes that the expectations reflected in such
forward-looking information are reasonable, it can give no
assurance that the expectations of any forward-looking information
will prove to be correct. Known and unknown risks, uncertainties,
and other factors which may cause the actual results and future
events to differ materially from those expressed or implied by such
forward-looking information. Such factors include but are not
limited to: compliance with extensive government regulations;
financial abilities; the ability to develop the Miller deposit;
domestic and foreign laws and regulations adversely affecting the
Company’s business and results of operations; the impact of
COVID-19; and general business, economic, competitive, political,
and social uncertainties. Accordingly, readers should not place
undue reliance on the forward-looking information contained in this
press release. Except as required by law, the Company disclaims any
intention and assumes no obligation to update or revise any
forward-looking information to reflect actual results, whether as a
result of new information, future events, changes in assumptions,
changes in factors affecting such forward-looking information or
otherwise.
Neither TSX Venture Exchange nor its
Regulation Services Provider (as that term is defined in the
policies of the TSX Venture Exchange) accepts responsibility for
the adequacy or accuracy of this release.
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